VEF-1200-GB Molten Salt Reactor with Integrated Glovebox for Air-Sensitive Materials
The VEF-1200-GB is engineered for laboratory processes involving molten salts that require strict atmosphere control to prevent contamination by moisture or oxygen. It integrates a high-temperature molten salt reactor with a glovebox, enabling safe manipulation of air-sensitive materials while maintaining an inert environment. This setup is ideal for research and development tasks where precise temperature control and atmosphere integrity are critical.
The reactor features a hermetically sealed dual quartz chamber design that ensures safety and preserves glovebox integrity. It can operate continuously at temperatures up to 1100°C with a heating zone of 240 mm diameter by 245 mm height, suitable for sample volumes up to approximately 3 liters. The glovebox maintains moisture and oxygen levels below 1 ppm, providing an ultra-clean environment for sensitive experiments.
Wichtigste Merkmale
- Maximum continuous operating temperature of 1100°C with controlled heating rate up to 20°C/min.
- Dual quartz chambers (inner Ø200×425 mm, outer Ø220×425 mm) for enhanced safety and atmosphere isolation.
- Hermetic chamber with gas inlet/outlet ports and optional in-situ temperature measurement capability.
- Integrated VGB-6 glovebox maintaining moisture and oxygen below 1 ppm for air-sensitive handling.
- Three-electrode system feedthroughs compatible with Ø6 mm electrodes (electrodes not included).
- PID temperature controller with ±1°C accuracy and programmable segments for precise thermal processes.
- Water-cooled dual-tube flanges to maintain vacuum flange integrity during operation.
Technische Daten
| Parameter | Spezifikation |
|---|---|
| Maximale Betriebstemperatur | 1100°C continuous |
| Erwärmungsgeschwindigkeit | Up to 20°C/min |
| Heating Zone Dimensions | Ø240 × 245 mm (11 L volume) |
| Quartz Inner Chamber | Ø200 × 425 mm, 13.2 L nominal capacity |
| Quartz Outer Chamber | Ø220 × 425 mm |
| Crucible | Quartz, Ø120 × 114 × 150 mm |
| Electrode Feedthroughs | Three 1/8″ copper feedthroughs for Ø6 mm electrodes (not included) |
| Thermal Block | Alumina foam, Ø190 × 60 mm height |
| Pressure Limit | Less than 3 psig |
| Glovebox Model | VGB-6 single chamber, moisture and oxygen < 1 ppm |
| Power Supply (Molten Salt Reactor) | 208-240 VAC, single phase, 50/60 Hz, 30 A, 4 kVA |
| Power Supply (Glovebox) | 120 VAC, single phase, 50/60 Hz, 15 A or 208-240 VAC, single phase, 50/60 Hz, 10 A |
| Temperaturregler | PID with auto-tune, ±1°C accuracy, 50 programmable segments |
| Thermocouples | K type for furnace control; optional K type for in-situ monitoring |
| Kühlung | Water cooling required for vacuum flange; water chiller optional |
Typische Anwendungsbereiche
This reactor system is suited for molten salt electrolysis, synthesis, and processing of air-sensitive materials under inert atmosphere. It supports electrochemical studies using three-electrode setups and precise thermal treatments requiring controlled atmosphere and temperature stability.
Hinweise zur Konfiguration und zum Betrieb
The system includes the molten salt reactor with integrated glovebox and necessary power cords; however, electrodes and water chiller are optional. Water cooling is mandatory for vacuum flange operation to maintain system integrity. Users should ensure proper handling of air-sensitive materials within the glovebox environment and follow safety protocols for high-temperature operation.
