AM-SP02-GB Automated Solid Phase Synthesis Platform in Glovebox for Sulfide and Halide Electrolytes with Integrated Dosing, Mixing, and Pellet Pressing
The AM-SP02-GB platform addresses the challenge of synthesizing air-sensitive sulfide and halide electrolytes by providing a fully automated solid-state synthesis workflow within a controlled glovebox environment. This system is tailored for researchers requiring precise handling and processing of moisture- and oxygen-sensitive powders, ensuring sample integrity throughout preparation.
The workstation integrates multiple processing stages: automatic dosing of starting powders, centrifugal dry mixing or ball milling, powder transfer via vibration, and pellet pressing. A robotic arm seamlessly transports samples between stations, enabling unattended operation and consistent sample preparation. Optional integration of an automatic tube furnace allows for pellet sintering within the glovebox.
Key Features
- Automatic dosing station with 10 channels for precise powder delivery.
- Centrifugal dry mixer/ball mill station equipped with 6 jars, each 15 ml capacity.
- Vibrating station facilitates powder transfer into pellet pressing dies.
- Pellet pressing station capable of up to 8 tons pressing force, with 6 dies of 10 mm inner diameter.
- Robotic arm automates sample movement between processing stations.
- Optional automatic tube furnace for in-glovebox pellet sintering.
- Operates within a three-chamber glovebox maintaining inert atmosphere for air-sensitive materials.
Technical Specifications
| Parameter | Specification |
|---|---|
| Power Supply | AC 220V ±10%, Single Phase, 50 Hz |
| Total Power Consumption | 5 kW (Glovebox: 1.5 kW; Machine: 3.5 kW) |
| Operating Temperature | 25ºC ±3% |
| Relative Humidity | 30 – 90% RH |
| Dosing Channels | 10 powder channels |
| Mixer Jars | 6 jars, 15 ml each |
| Pellet Pressing Force | Up to 8 tons |
| Pellet Die Size | 6 dies, 10 mm inner diameter |
| Certifications | CE certified; NRTL certification optional |
Typical Applications
This platform is ideal for automated synthesis of sulfide and halide solid electrolytes used in advanced battery research. It supports preparation of air-sensitive materials requiring strict inert atmosphere control, enabling consistent powder mixing, milling, and pellet formation for subsequent electrochemical testing or sintering.
Configuration & Operating Notes
The system includes a three-chamber glovebox housing all processing stations and a robotic arm for automated sample transfer. An optional tube furnace can be integrated for pellet sintering within the glovebox. The platform requires a controlled environment at 25ºC ±3% and 30-90% relative humidity or a dry room with dew point below -50ºC if operated without the glovebox. CE certification ensures compliance with safety standards; NRTL certification is available upon request.
