GSL-1100X-RC Superalloy High Pressure Hydrothermal Reactor with 65ml & 100ml Capacity, Up to 1100°C and 4 MPa Pressure
The GSL-1100X-RC reactor is engineered for hydrothermal synthesis and heat treatment of advanced materials requiring high temperature and controlled oxygen or inert gas pressure environments. Its nickel-based superalloy construction provides superior creep strength and oxidation resistance, enabling safe operation at temperatures up to 1100°C and pressures up to 4 MPa. This makes it particularly suitable for processing samples under elevated oxygen pressures where material stability is critical.
The reactor vessel is available in two capacities, 65 mL and 100 mL, with precise digital temperature control featuring 30 programmable segments and ±1°C accuracy. A solenoid valve mounted on the flange automatically relieves pressure when it reaches a preset alarm threshold, enhancing operational safety. Real-time monitoring of temperature and pressure is supported via included software, with optional PC control compatible with LabVIEW for advanced process management.
Wichtigste Merkmale
- Pressure vessel made from Ni-base superalloy for high creep strength and oxidation resistance.
- Operating temperature range from room temperature to 1100°C with digital temperature controller.
- Pressure capability up to 4 MPa at 1100°C under oxygen or inert gas atmospheres.
- Solenoid valve on flange for automatic pressure relief at preset limits (default 15 MPa max).
- Real-time temperature and pressure monitoring software included; optional PC control module available.
- Two vessel sizes: 65 mL (55 mm OD x 20 mm ID x 214 mm height) and 100 mL (65 mm OD x 25 mm ID x 210 mm height).
- Omega K-type thermocouple with high-temperature tolerance connector for accurate temperature measurement.
Technische Daten
| Parameter | Spezifikation |
|---|---|
| Modell | GSL-1100X-RC |
| Pressure Vessel Material | Ni-Based Superalloy |
| Vessel Capacities | 65 mL and 100 mL |
| Vessel Dimensions (65 mL) | 55 mm OD x 20 mm ID x 214 mm height |
| Vessel Dimensions (100 mL) | 65 mm OD x 25 mm ID x 210 mm height |
| Betriebstemperaturbereich | Room Temperature to 1100°C |
| Temperaturregler | Digital, 30 programmable segments, ±1°C accuracy |
| Maximum Pressure at 1100°C | 4 MPa (65 mL), 4 MPa (100 mL) |
| Pressure Sensor | Precision high-pressure sensor, up to 250 bars measurement range |
| Pressure Relief Valve | Solenoid valve with 15 MPa max pressure relief (default) |
| Thermoelement | Omega 3 mm OD K Type with high-temperature tolerance connector |
| Stromversorgung | AC 208–240 V, Single Phase, 2 kW |
Typische Anwendungsbereiche
This reactor is ideal for hydrothermal synthesis of advanced materials, including crystal growth and heat treatment under controlled oxygen or inert atmospheres. It is well suited for research requiring precise temperature and pressure control up to 1100°C and 4 MPa, such as preparation of oxides, catalysts, and other functional materials.
Hinweise zur Konfiguration und zum Betrieb
The reactor includes a solenoid valve for automatic pressure relief and a precision pressure sensor. It is recommended to use a two-stage pressure regulator on the gas supply to limit pressure below 3 PSI for safety. Samples must be loaded inside small quartz or alumina boats; direct contact with the vessel is not advised to prevent damage. Gold or nickel foil can be used to wrap crucibles to reduce contamination. The processing tube is consumable and replaceable. For safety, the reactor and furnace should be operated inside an explosion-proof enclosure. Proper torque application on flange bolts is critical to avoid damage; a torque wrench is recommended.
