GSL-1100X-RC Superalloy High-Pressure Hydrothermal Reactor with 1100°C Max Temperature and 4 MPa Oxygen/Inert Gas Pressure
The GSL-1100X-RC reactor is engineered for hydrothermal synthesis and heat treatment of materials requiring elevated temperatures and controlled high-pressure oxygen or inert gas environments. Its Ni-based superalloy construction provides superior creep strength and oxidation resistance, enabling reliable operation at temperatures up to 1100°C and pressures up to 4 MPa. This makes it particularly suitable for preparing advanced materials and conducting experiments under aggressive oxidative conditions.
Equipped with a solenoid valve integrated into the flange, the reactor allows automatic pressure relief to maintain safe operating conditions. The system includes digital temperature control with 30 programmable segments and precision pressure sensors for real-time monitoring. Two vessel sizes are available—65 mL and 100 mL—each designed with an air-cooled flange and aluminum heat radiator to optimize thermal management.
Wichtigste Merkmale
- Pressure vessel made from Ni-based superalloy for high creep strength and oxidation resistance.
- Maximum operating temperature of 1100°C and pressure up to 4 MPa under oxygen or inert gas.
- Automatic pressure relief via solenoid valve installed on the flange for enhanced safety.
- Digital temperature controller with 30-segment programmable heating and ±1°C accuracy.
- Real-time temperature and pressure monitoring software included for precise process control.
- Available vessel capacities: 65 mL (55 mm OD x 20 mm ID) and 100 mL (65 mm OD x 25 mm ID).
- Omega K-type thermocouple with high-temperature tolerance and air-cooled flange design.
Technische Daten
| Parameter | Spezifikation |
|---|---|
| Pressure Vessel Material | Ni-based Superalloy |
| Vessel Capacities and Dimensions | 65 mL: 55 mm OD x 20 mm ID x 214 mm height; 100 mL: 65 mm OD x 25 mm ID x 210 mm height |
| Höchsttemperatur | 1100°C |
| Maximaler Druck | 4 MPa at 1100°C (oxygen or inert gas) |
| Temperaturregler | Digital, 30 programmable segments, ±1°C accuracy |
| Thermoelement | Omega K-type, 3 mm OD, high-temperature connector (220°C tolerance) |
| Pressure Sensor | Precision sensor with measurement range up to 250 bars |
| Pressure Relief Valve | Solenoid valve with 15 MPa max relief pressure (manual needle valve for >15 MPa) |
| Stromversorgung | AC 208–240 V, Single Phase, 2 kW |
Typische Anwendungsbereiche
This reactor is ideal for hydrothermal synthesis of advanced materials requiring high temperature and oxygen-rich or inert atmospheres. It is frequently used for heat treatment of samples under elevated oxygen pressure and can also function as a steam generator for specialized processes.
Hinweise zur Konfiguration und zum Betrieb
The reactor includes a SS316 needle valve with 1/4″ pipe connector and pressure gauge. Two copper gaskets (48 mm O.D.) are supplied as consumables. Optional accessories include torque wrenches to ensure proper flange bolt tightening and replacement liners made from various materials to suit different sample growth requirements.
For safety, the reactor and furnace must be operated inside an explosion-proof enclosure when under high pressure. Users must never face the top flange without protection. A two-stage pressure regulator should be installed on the gas supply to limit pressure below 3 PSI. Samples must be loaded in quartz or alumina boats; direct contact with the vessel is prohibited to avoid damage. Wrapping crucibles with gold or nickel foil is recommended to minimize contamination.
