AM-SP02-GB Automated Solid Phase Synthesis Platform in Glovebox for Sulfide and Halide Electrolytes
The AM-SP02-GB is engineered to facilitate the automated synthesis of air-sensitive sulfide and halide electrolyte materials within a controlled glovebox atmosphere. This platform addresses the challenges of handling moisture- and oxygen-sensitive powders by integrating multiple synthesis steps into a seamless automated workflow, minimizing exposure and contamination risks.
The system automates the entire process from precise powder dosing through mixing and milling to pellet pressing. A robotic arm transfers samples between stations, ensuring consistent handling and reproducibility. The glovebox environment maintains inert conditions suitable for sensitive materials, with an option to add an automatic tube furnace for pellet sintering.
Key Features
- Automatic dosing station with 10 channels for precise powder element delivery.
- Centrifugal dry mixer/ball mill station equipped with six 15 ml jars for thorough mixing.
- Vibrating station to transfer mixed powders into pellet pressing dies efficiently.
- Pellet pressing station capable of applying up to 8 tons of force, with six 10 mm internal diameter dies.
- Robotic arm automates sample movement between dosing, mixing, vibrating, and pressing stations.
- Glovebox integration ensures an inert atmosphere for handling air-sensitive materials.
- Optional automatic tube furnace for sintering pellets within the glovebox environment.
Technical Specifications
| Parameter | Specification |
|---|---|
| Power Supply | AC 220V ±10%, Single Phase, 50 Hz |
| Total Power Consumption | 5 kW (Glovebox: 1.5 kW, Machine: 3.5 kW) |
| Dosing Channels | 10 channels for starting powder elements |
| Mixer/Mill Jars | 6 jars, each 15 ml capacity |
| Pellet Pressing Force | Maximum 8 tons |
| Pellet Die Size | 6 dies, 10 mm internal diameter |
| Operating Environment | Glovebox atmosphere or dry room with dew point below -50°C |
| Temperature Range | 25°C ±3% |
| Humidity Range | 30% – 90% RH |
| Certifications | CE certified; NRTL certification available on request |
Typical Applications
This platform is ideal for research and development of sulfide and halide solid electrolytes used in advanced battery technologies. It supports synthesis workflows requiring strict moisture and oxygen exclusion, such as preparation of air-sensitive solid-state electrolyte powders and pellet fabrication for electrochemical testing.
Configuration & Operating Notes
The system includes an integrated robotic arm for automated sample transfer between stations. Optional accessories include an automatic tube furnace for in-glovebox pellet sintering. Users should maintain the glovebox environment or a dry room with dew point below -50°C to ensure material stability. Proper training on glovebox operation and safety protocols for handling air-sensitive powders is recommended.
