GSL-1100X-RC-NI300 300 mL Ni-Based Superalloy High-Pressure Reactor for Hydrothermal Synthesis up to 1100°C and 3 MPa
The GSL-1100X-RC-NI300 reactor is engineered for hydrothermal synthesis and heat treatment of materials requiring high temperature and controlled high-pressure oxygen or inert atmospheres. Its 300 mL capacity vessel, made from a nickel-based superalloy (GH747), provides exceptional creep strength and oxidation resistance, enabling operations at temperatures up to 1100°C and pressures up to 3 MPa. This makes it particularly suitable for advanced material preparation and crystal growth under challenging conditions.
The reactor integrates a solenoid valve on the flange for automatic pressure relief, enhancing operational safety by preventing overpressure. Temperature control and pressure monitoring software facilitate remote operation and precise process control. The system includes alarms and interlocks for over-temperature and overpressure conditions, ensuring safe and reliable use. The reactor vessel is consumable and can be replaced as needed, with options for liners to minimize contamination depending on the material processed.
주요 기능
- Ni-based superalloy GH747 construction for high creep strength and oxidation resistance at elevated temperatures.
- Operating temperature up to 1100°C (short term) and continuous operation up to 1000°C.
- Pressure capability up to 16.5 MPa at ≤800°C, decreasing to 3 MPa at 1100°C.
- Solenoid valve for automatic pressure relief and integrated high-pressure sensor with alarm settings.
- Temperature controller with 30 programmable segments and ±1°C accuracy.
- Remote control capability via included temperature and pressure monitoring software.
- Includes SS316 needle valve with pressure gauge and consumable copper gaskets.
기술 사양
| 매개변수 | 사양 |
|---|---|
| 모델 | GSL-1100X-RC-NI300 |
| Reactor Capacity | 300 mL |
| 재료 | Ni-based superalloy GH747 |
| Reactor Dimensions | 70 mm OD × 35 mm ID × 326 mm H |
| 최고 기온 | 1100°C (short term), ≤1000°C continuous |
| 최대 압력 | 16.5 MPa ≤800°C, 10 MPa ≤900°C, 5 MPa ≤1000°C, 3 MPa ≤1100°C |
| Heating Element | Fe-Cr-Al alloy |
| Thermocouple | K-type, Omega 3 mm OD with high-temp connector |
| Heating/Cooling Rate | ≤10°C/min |
| Power Supply | 208-240 VAC, 50/60 Hz, single phase, 1.5 kW |
| Pressure Sensor Range | Up to 25 MPa (250 bar) |
| Control Software | Included for temperature and pressure monitoring; optional PC control software available |
대표적인 적용 분야
Ideal for hydrothermal crystal growth, heat treatment under high oxygen pressure, and synthesis of advanced materials requiring precise temperature and pressure control in corrosive or oxidizing environments.
구성 및 작동 안내
The reactor includes a solenoid valve for automatic pressure relief and a SS316 needle valve with pressure gauge. Consumable copper gaskets are supplied, with replacements available. The vessel is consumable and should be replaced as needed. Use of liners such as gold or nickel foil is recommended to reduce contamination. The high-pressure vessel must be operated inside an explosion-proof enclosure or isolated room for safety. Over-tightening flange screws should be avoided; proper torque tools are recommended. Manual pressure relief valves must be used for venting to protect the solenoid valve from contamination. Remote operation is advised to enhance safety during high-pressure use.
