VBF-1200S-MS Three-Electrode Molten Salt Reactor with 4″ Quartz Vessel for Electrolysis up to 1100°C
The VBF-1200S-MS is engineered to facilitate advanced molten salt electrolysis experiments requiring stable high-temperature environments and precise electrochemical control. It is particularly suited for laboratory-scale research involving molten salt reactions, enabling detailed studies of electrochemical processes under controlled atmospheres and temperatures up to 1100°C.
This system integrates a benchtop furnace designed to accommodate a 4-inch outer diameter quartz reaction vessel, providing a chemically inert and thermally stable environment. The reactor includes a three-electrode configuration for accurate electrochemical measurements, along with gas inlet and outlet ports to allow controlled atmosphere conditions. Temperature is monitored in situ by a type K thermocouple embedded within the reactor assembly, with a digital PID controller ensuring precise temperature regulation and programmable heating profiles.
Wichtigste Merkmale
- Benchtop furnace compatible with a 4″ quartz reaction vessel rated for continuous operation below 1100°C.
- Three-electrode electrochemical system enabling detailed molten salt electrolysis studies.
- Gas inlet and outlet ports for atmosphere control during experiments.
- In-situ type K thermocouple for accurate temperature measurement within the reaction chamber.
- Digital temperature controller with PID and auto-tune functions, supporting up to 30 programmable segments.
- Stainless steel 316 hermetic flange with six 1/4″ compression fittings for secure connections.
- Optional alumina crucibles available in multiple sizes to accommodate various sample volumes.
Technische Daten
| Parameter | Spezifikation |
|---|---|
| Stromversorgung | AC 110-120V, 50/60Hz, 20A, 1.5KVA or AC 208-240V, 50/60Hz, 15A, 1.8KVA |
| Maximum Operating Temperature | Continuous operation below 1100°C |
| Maximum Heating Rate | 20 °C/min |
| Maximaler Druck | 3 psig |
| Reaction Vessel | Quartz tube 100 mm OD × 94 mm ID × 300 mm length, 1.7 L capacity |
| Flange | SS 316 hermetic flange with six 1/4″ compression tube fittings |
| Electrodes | Three-electrode system with Ø3 mm copper sheathed electrodes inside Ø6 mm alumina tubes, rated up to 55A |
| Temperatursensor | In-situ type K thermocouple |
| Heizbereich | Ø120 mm ID × 200 mm height |
| Temperaturregler | Digital PID controller with ±1°C accuracy, auto-tune, 30 programmable segments, overheating and thermocouple failure protection |
| Optional DC Power Supply | Programmable up to 30 V DC, 100 A max (sold separately) |
Typische Anwendungsbereiche
Ideal for molten salt electrolysis research, materials synthesis under controlled atmospheres, and high-temperature electrochemical studies involving molten salts. Suitable for academic and industrial laboratories focusing on energy storage, metallurgy, and advanced materials development.
Hinweise zur Konfiguration und zum Betrieb
The system includes the quartz reaction vessel, stainless steel hermetic flange, three-electrode assembly connections, and integrated temperature controller. Electrodes and optional alumina crucibles are not included and must be sourced separately. The optional programmable DC power supply enhances electrochemical control but is sold separately. Users should ensure proper gas handling and safety protocols when operating under pressurized or reactive atmospheres.
